Derivatization in mass spectrometry--8. Soft ionization mass spectrometry of small molecules (Q28242166)

European Journal of Mass Spectrometry

Europe PubMed Central

title

Derivatization in mass spectrometry--8. Soft ionization mass spectrometry of small molecules (English)

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Vladimir G Zaikin

1

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John M Halket

series ordinal

2

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language of work or name

English

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publication date

2006

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published in

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volume

12

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issue

2

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page(s)

79-115

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Derivatization in mass spectrometry-3. Alkylation (arylation).

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Review: derivatization in mass spectrometry--5. Specific derivatization of monofunctional compounds

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Review: derivatization in mass spectrometry-6. Formation of mixed derivatives of polyfunctional compounds

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Derivatization in mass spectrometry --7. On-line derivatisation/degradation

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Protein and polymer analyses up tom/z 100 000 by laser ionization time-of-flight mass spectrometry

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Electrospray ion source. Another variation on the free-jet theme

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Optimization of the atmospheric pressure chemical ionization liquid chromatography mass spectrometry interface

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Chemical derivatization and mass spectral libraries in metabolic profiling by GC/MS and LC/MS/MS.

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Derivatization of small biomolecules for optimized matrix-assisted laser desorption/ionization mass spectrometry

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Analysis of sialo-N-glycans in glycoproteins as 1-phenyl-3-methyl-5-pyrazolone derivatives by capillary electrophoresis

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Reversed-phase liquid chromatographic method for the analysis of aminoglycoside antibiotics using pre-column derivatization with phenylisocyanate

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Assay of histamine by nano-liquid chromatography/tandem mass spectrometry with a packed nanoelectrospray emitter

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Derivatisation for liquid chromatography/electrospray mass spectrometry: synthesis of pyridinium compounds and their amine and carboxylic acid derivatives

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Determination of the herbicide amitrole in water with pre-column derivatization, liquid chromatography and tandem mass spectrometry

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Derivatization for liquid chromatography/electrospray mass spectrometry: synthesis of tris(trimethoxyphenyl)phosphonium compounds and their derivatives of amine and carboxylic acids.

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Qualitative and quantitative analysis of small amine molecules by MALDI-TOF mass spectrometry through charge derivatization.

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On-line on-chip post-column derivatisation reactions for pre-ionisation of analytes and cluster analysis in gradient micro-liquid chromatography/electrospray mass spectrometry.

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Single bead and hard tag decoding using accurate isotopic difference target analysis-encoded combinatorial libraries

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On-line determination of carboxylic acids, aldehydes and ketones by high-performance liquid chromatography-diode array detection-atmospheric pressure chemical ionisation mass spectrometry after derivatization with 2-nitrophenylhydrazine

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Derivatisation of carboxylic acid groups in pharmaceuticals for enhanced detection using liquid chromatography with electrospray ionisation tandem mass spectrometry

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Tandem mass spectrometry in the study of fatty acids, bile acids, and steroids

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Derivatization to improve thermospray HPLC/MS sensitivity for the determination of prostaglandins and thromboxane B2.

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Analysis of isomeric long-chain hydroxy fatty acids by tandem mass spectrometry: application to the diagnosis of long-chain 3-hydroxyacyl CoA dehydrogenase deficiency

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Targeted lipidomics using electron capture atmospheric pressure chemical ionization mass spectrometry

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Analysis of amino acids as formamidene butyl esters by electrospray ionization tandem mass spectrometry

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Quantification of glutamine in dried blood spots and plasma by tandem mass spectrometry for the biochemical diagnosis and monitoring of ornithine transcarbamylase deficiency

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Fragmentation pathway for glutamine identification: loss of 73 Da from dimethylformamidine glutamine isobutyl ester

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Determination of carbocysteine in human plasma by liquid chromatography/tandem mass spectrometry employing precolumn derivatization

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Distinction of Leu and Ile Using a Ruthenium(II) complex by MALDI-LIFT-TOF/TOF-MS analysis.

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Acid hydrolysis of silk fibroins and determination of the enrichment of isotopically labeled amino acids using precolumn derivatization and high-performance liquid chromatography-electrospray ionization-mass spectrometry

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Derivatization of amino acids with N,N-dimethyl-2,4-dinitro-5-fluorobenzylamine for liquid chromatography/electrospray ionization mass spectrometry

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Sensitivity improvement of amino acids by N-terminal diisopropyloxyphosphorylation in electrospray ionization mass spectrometry

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ESI mass spectrometry of amino acid trimethylsilylethyl esters.

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Determination of arginine and asymmetric dimethylarginine (ADMA) in human plasma by liquid chromatography/mass spectrometry with the isotope dilution technique

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Chirality determination of unusual amino acids using precolumn derivatization and liquid chromatography-electrospray ionization mass spectrometry

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Chiral analysis by electrospray ionization mass spectrometry/mass spectrometry. 2. Determination of enantiomeric excess of amino acids.

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Enantiomeric separation of amino acids derivatized with 7-fluoro-4-nitrobenzoxadiazole by capillary liquid chromatography/tandem mass spectrometry

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Derivatization LC/MS for the simultaneous determination of fatty alcohol and alcohol ethoxylate surfactants in water and wastewater samples

21 January 2018

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Nanoelectrospray mass spectrometry and precursor ion monitoring for quantitative steroid analysis and attomole sensitivity

21 January 2018

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Liquid chromatography/electron capture atmospheric pressure chemical ionization/mass spectrometry: analysis of pentafluorobenzyl derivatives of biomolecules and drugs in the attomole range

21 January 2018

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Investigation of amine and polyol functionality in extracts of polyurethane wound management dressings using MALDI-MS.

21 January 2018

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Use of S-pentafluorophenyl tris(2,4,6-trimethoxyphenyl)phosphonium acetate bromide and (4-hydrazino-4-oxobutyl) [tris(2,4,6-trimethoxyphenyl)phosphonium bromide for the derivatization of alcohols, aldehydes and ketones for detection by liquid chroma

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Derivatization for LC-electrospray ionization-MS: a tool for improving reversed-phase separation and ESI responses of bases, ribosides, and intact nucleotides

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Strategies for the liquid chromatographic-mass spectrometric analysis of non-polar compounds

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Electrospray tandem mass spectrometric study of ferrocene carbamate ester derivatives of saturated primary, secondary and tertiary alcohols

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Liquid chromatography with post-column electrochemical treatment and mass spectrometric detection of non-polar compounds

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Determination of brassinosteroids in the sub-femtomolar range using dansyl-3-aminophenylboronate derivatization and electrospray mass spectrometry

21 January 2018

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Derivatization of ethinylestradiol with dansyl chloride to enhance electrospray ionization: application in trace analysis of ethinylestradiol in rhesus monkey plasma

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Quantitation of 17alpha-ethinylestradiol in aquatic samples using liquid-liquid phase extraction, dansyl derivatization, and liquid chromatography/positive electrospray tandem mass spectrometry

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Trace level quantification of deuterated 17beta-estradiol and estrone in ovariectomized mouse plasma and brain using liquid chromatography/tandem mass spectrometry following dansylation reaction

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Structure Elucidation of 2,4-Dinitrophenylhydrazone Derivatives of Carbonyl Compounds in Ambient Air by HPLC/MS and Multiple MS/MS Using Atmospheric Chemical Ionization in the Negative Ion Mode

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Derivatisation for the characterisation of neutral oxosteroids by electrospray and matrix-assisted laser desorption/ionisation tandem mass spectrometry: the Girard P derivative.

21 January 2018

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Detection and characterization of 20-oxosteroids in rat brains using LC-electron capture APCI-MS after derivatization with 2-nitro-4-trifluoromethylphenylhydrazine

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A high-performance liquid chromatography/tandem mass spectrometric screening method for eight synthetic corticosteroids in bovine feces and the simultaneous differentiation between dexamethasone and betamethasone.

21 January 2018

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Liquid Chromatography Analysis of Carbonyl (2,4-Dinitrophenyl)hydrazones with Detection by Diode Array Ultraviolet Spectroscopy and by Atmospheric Pressure Negative Chemical Ionization Mass Spectrometry

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Qualitative and quantitative analysis of carbonyl compounds in ambient air samples by use of an HPLC-MS(n) method

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Atmospheric pressure chemical ionization mass spectrometry of aldehydes in biological matrices

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HPLC-MS determination of the oxidation products of the reaction between alpha- and beta-pinene and OH radicals

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Determination of patterns of biologically relevant aldehydes in exhaled breath condensate of healthy subjects by liquid chromatography/atmospheric chemical ionization tandem mass spectrometry.

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Method optimization for the determination of carbonyl compounds in disinfected water by DNPH derivatization and LC-ESI-MS-MS.

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Analysis of oxysterols by electrospray tandem mass spectrometry

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Ketosteroid profiling using Girard T derivatives and electrospray ionization tandem mass spectrometry: direct plasma analysis of androstenedione, 17-hydroxyprogesterone and cortisol

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Rapid monitoring assay of congenital adrenal hyperplasia with microbore high-performance liquid chromatography/electrospray ionization tandem mass spectrometry from dried blood spots

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Derivatization of carbohydrates for chromatographic, electrophoretic and mass spectrometric structure analysis

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Matrix-assisted laser desorption/ionization mass spectrometry of carbohydrates

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Mass spectrometry of oligosaccharides.

21 January 2018

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Size exclusion chromatography/mass spectrometry applied to the analysis of polysaccharides

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Incremented alkyl derivatives enhance collision induced glycosidic bond cleavage in mass spectrometry of disaccharides

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Derivatization of small oligosaccharides prior to analysis by matrix-assisted laser desorption/ionization using glycidyltrimethylammonium chloride and Girard's reagent T.

21 January 2018

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Analysis of N-acetylated hexosamine monosaccharides by ferrocenyl boronation and tandem electrospray ionization mass spectrometry

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Analysis of neutral isomeric low molecular weight carbohydrates using ferrocenyl boronate derivatization and tandem electrospray mass spectrometry

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Oligosaccharide profiling: the facile detection of mono-, di- and oligosaccharides by electrospray orthogonal time-of-flight mass spectrometry using 3-aminophenylboronic acid derivatization

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Investigation of different combinations of derivatization, separation methods and electrospray ionization mass spectrometry for standard oligosaccharides and glycans from ovalbumin

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Characterization of carbohydrates using a combination of derivatization, high-performance liquid chromatography and mass spectrometry

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Rapid analysis of O-acetylated neuraminic acids by matrix assisted laser desorption/ionization time-of-flight mass spectrometry

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Specific distribution of sialic acids in animal tissues as examined by LC-ESI-MS after derivatization with 1,2-diamino-4,5-methylenedioxybenzene

21 January 2018

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New sialic acids from biological sources identified by a comprehensive and sensitive approach: liquid chromatography-electrospray ionization-mass spectrometry (LC-ESI-MS) of SIA quinoxalinones

21 January 2018

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A new LC/MS-method for the quantitation of acrylamide based on a stable isotope dilution assay and derivatization with 2-mercaptobenzoic acid. Comparison with two GC/MS methods

21 January 2018

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Total structure characterization of unsaturated acidic phospholipids provided by vicinal di-hydroxylation of fatty acid double bonds and negative electrospray ionization mass spectrometry

21 January 2018

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Application of 4-(4-nitrophenyl)-1,2,4-triazoline-3,5-dione to analysis of 25-hydroxyvitamin D3 in human plasma by liquid chromatography/electron capture atmospheric pressure chemical ionization-mass spectrometry

21 January 2018

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Trapping 4-fluorobenzyl chloride in human plasma with chemical derivatization followed by quantitative bioanalysis using high-performance liquid chromatography/tandem mass spectrometry

21 January 2018

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High-performance liquid chromatography-based determination of total isothiocyanate levels in human plasma: application to studies with 2-phenethyl isothiocyanate

21 January 2018

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Quantitative determination of dithiocarbamates in human plasma, serum, erythrocytes and urine: pharmacokinetics of broccoli sprout isothiocyanates in humans

21 January 2018

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Determination of phenethyl isothiocyanate in human plasma and urine by ammonia derivatization and liquid chromatography–tandem mass spectrometry

21 January 2018

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Ferrocenoyl piperazide as derivatizing agent for the analysis of isocyanates and related compounds using liquid chromatography/electrochemistry/mass spectrometry (LC/EC/MS).

21 January 2018

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4-Nitro-7-piperazino-2,1,3-benzoxadiazole as a reagent for monitoring of airborne isocyanates by liquid chromatography

21 January 2018

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Atmospheric pressure photoionization: an ionization method for liquid chromatography-mass spectrometry

21 January 2018

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Atmospheric pressure photoionization mass spectrometry

21 January 2018

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Determination of aldehydes and ketones using derivatization with 2,4-dinitrophenylhydrazine and liquid chromatography-atmospheric pressure photoionization-mass spectrometry

21 January 2018

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On-line derivatization for resonance-enhanced multiphoton ionization time-of-flight mass spectrometry: detection of aliphatic aldehydes and amines via reactive coupling of aromatic photo ionization labels

21 January 2018

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